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The expression (9.115) represents the difference between measured powers under matched and unmatched cases. Table 9.7 lists the calculated results in dB. It can be seen that in the eleventh row of Table 9.7 where RS = 50 , XS = 0 , the impedance matching condition is satis ed so that the impedance of the tested point matches that of the spectrum analyzer. This results in the measured power, PL, being equal to the expected power, Po, as shown in matched case (a). In general, in the unmatched * case (b), the measured power, PL , will deviate from the expected power, Po, by a certain amount. The deviation becomes signi cant when the impedance is far from a matched condition. The power reading in the unmatched case is always lower than the power reading under the impedance matched case. In some cases the difference is horrible! For instance, as shown in the tenth row of Table 9.7 where the impedance of DTU is ZS = 10 + j10kW while the input impedance of power meter or spectrum analyzer is 50 , the difference is 47 dB! * Figure 9.21 plots the calculated power ratio, PL /Po, vs. impedance of the DTU, ZS. This waterfall diagram may give you an intuitive feeling for the inaccuracy of power measure due to the unmatched impedance.

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CREATE TABLE RawCategory ( RawCategoryID CHAR(1), CategoryName VARCHAR(25) ) INSERT RawCategory (RawCategoryID, CategoryName) VALUES ( X , Sci-Fi ) INSERT RawCategory (RawCategoryID, CategoryName) VALUES ( Y , Philosophy ) INSERT RawCategory (RawCategoryID, CategoryName) VALUES ( Z , Zoology ) -- including data outside the aggregate function or group by SELECT Category, CategoryName, Sum(Amount) as [Sum], Avg(Amount) as [Avg], Min(Amount) as [Min], Max(Amount) as [Max] FROM RawData R JOIN RawCategory C ON R.Category = C.RawCategoryID GROUP BY Category

and is the contact angle measured between crystal and the solid surface on which nucleation occurs Energetically, heterogeneous nucleation will always be preferred, con rming the importance of the substrate in the phase transformation of solution deposited lms Brinker and Scherer1,64 have carried out a detailed analysis of the impact that the physical factors noted above can have on the free energy of the amorphous material This analysis leads to the ability to predict the driving force associated with the phase transformation into the crystalline state A typical approach to this analysis is shown below for estimating the contribution of residual hydroxyl species If the chemical synthesis of SiO2 is chosen for consideration, the role of hydroxyl species on free energy may be estimated from Si (OH )4 SiO2 + 2H 2O; G = 14.

1 m

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9 kJ mol Therefore, as more hydroxyls are retained in the lm, the free energy of the lm is increased Assuming that condensation is not complete (frequently the case) and that 033 to 148 OH species per Si are retained, the OH contribution to free energy may be estimated at 12 55 kJ/mol Using reported values of surface area and skeletal density for solution-derived thin lms leads to values of 9 30 kJ/mol and 6 kJ/mol for these contributions to the free energy of the amorphous material, respectively Considering that the typical driving force for the transformation ( Gv) is in the range of 50 80 kJ/mol,15 it may be seen that the physical characteristics of the amorphous state can make substantial contributions to the driving force for the transformation.